Effect of different parameters on composition of volatile components of Myristica fragrans seeds extracted by hydrodistillation assisted by microwave and head-space solid-phase microextraction
Effect of different parameters on composition of volatile components of Myristica fragrans seeds extracted by hydrodistillation assisted by microwave.pdf
[en] Hydrodistillation assisted by microwave (HDAM) and Head space solid phase micro-extraction (HSSPME)
of Myristica fragrans houtt (MF) were investigated. A kinetic study was performed for MF
seeds using two techniques (HDAM: Hydrodistillation assisted by microwave and SDAM: steam
distillation assisted by microwave). The effect of the cryogenic grinding (CG) showed differences in
yields and composition of volatile oils compared to the simple grinding (SG). HDAM–SG (3.4%) and
SDAM–SG (2.55%) allowed extraction of substantial amounts of volatile oils in less time compared
with HDAM–CG (4.75%) and SDAM–CG (3.8%). The kinetic study (differential and accumulated
yields) of essential oil extraction was quantitatively and qualitatively performed showing a
significant variation of composition with the extraction time, especially for accumulated yields
such as sabinene (31.48–38.78%), α-pinene (12.74–14.09%) and β-pinene (10.01–12.11%). Similarly,
the HS-SPME–GC–MS analysis showed also a significant variation of MF seeds volatile composition
according some parameters as the type of fibre coating (PDMS: Polydimethylsiloxane and PDMS–
DVB: Polydimethylsiloxane divenylbenzene), particle size, grinding mode and the mass used. The
chemical groups (monoterpenoids, aliphatic and aromatic alcohols and esters) showed specific
behaviour in SPME analysis. SPME sampling parameters were optimized for these components.
Disciplines :
Agriculture & agronomy Chemistry
Author, co-author :
Bouchachia, C
Benkaci-Ali, F
Eppe, Gauthier ; Université de Liège > Département de chimie (sciences) > Chimie analytique inorganique
Scholl, Georges ; Université de Liège > Département de chimie (sciences) > Center for Analytical Research and Technology (CART)
Language :
English
Title :
Effect of different parameters on composition of volatile components of Myristica fragrans seeds extracted by hydrodistillation assisted by microwave and head-space solid-phase microextraction
Publication date :
May 2017
Journal title :
Journal of Essential Oil Research
ISSN :
1041-2905
Publisher :
Allured Publishing Corporation, Carol Stream, United States - Illinois
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